3EZ7

Partition Protein Apo form in space group I4122

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Detector technology	CCD
Collection date	2007-01-02
Detector	ADSC QUANTUM 4
Wavelength(s)	1.0, 1.26554, 1.26541, 1.3500
Spacegroup name	I 41 2 2
Unit cell lengths	145.300, 145.300, 126.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	57.770 - 2.920
R-factor	0.24
Rwork	0.240
R-free	0.28300
Structure solution method	MAD
RMSD bond length	0.010
RMSD bond angle	1.600
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	SOLVE
Refinement software	CNS (1.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	72.600
High resolution limit [Å]	2.920
Number of reflections	15343
<I/σ(I)>	9.4
Completeness [%]	99.0
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.6	298	Formate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K