3EZ6
Structure of parA-ADP complex:tetragonal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Detector technology | CCD |
Collection date | 2007-01-02 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 143.300, 143.300, 108.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 101.330 - 2.580 |
R-factor | 0.187 |
Rwork | 0.187 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ez2 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.400 |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 107.800 |
High resolution limit [Å] | 2.580 |
Number of reflections | 35970 |
<I/σ(I)> | 8.9 |
Completeness [%] | 99.0 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | PEG 6000, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |