3EYU
PFA1 Fab fragment complexed with Ror2(518-525)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.90 |
Spacegroup name | P 1 |
Unit cell lengths | 41.632, 42.632, 58.729 |
Unit cell angles | 96.09, 93.58, 91.71 |
Refinement procedure
Resolution | 21.290 - 2.710 |
R-factor | 0.18 |
Rwork | 0.177 |
R-free | 0.24800 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.246 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.290 | 2.778 |
High resolution limit [Å] | 2.710 | 2.709 |
Number of reflections | 9216 | |
Completeness [%] | 84.8 | 45.48 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 20% w/v PEG3350, 0.2 M LiCl, vapor diffusion, sitting drop, temperature 298K |