3EYM
Structure of Influenza Haemagglutinin in complex with an inhibitor of membrane fusion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-09-09 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97565 |
Spacegroup name | P 41 |
Unit cell lengths | 160.465, 160.464, 176.548 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.930 - 2.800 |
R-factor | 0.19709 |
Rwork | 0.197 |
R-free | 0.21711 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.473 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 129.000 | 2.930 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 103890 | |
Completeness [%] | 99.8 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | Ammonium citratre, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |