3EVR

Crystal structure of Calcium bound monomeric GCAMP2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Detector technology	CCD
Collection date	2008-04-12
Detector	ADSC QUANTUM 210
Wavelength(s)	1.0
Spacegroup name	P 41 21 2
Unit cell lengths	121.995, 121.995, 97.831
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.649 - 2.000
R-factor	0.1655
Rwork	0.163
R-free	0.19020
RMSD bond length	0.009
RMSD bond angle	1.137
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.070
High resolution limit [Å]	2.000	4.310	2.000
Rmerge	0.127	0.054	0.710
Number of reflections	50531
<I/σ(I)>	23.625
Completeness [%]	100.0	100	100
Redundancy	17.4	16.7	15.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1