3EVM
Crystal structure of the Mimivirus NDK +Kpn-N62L-R107G triple mutant complexed with dCDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION ENHANCE ULTRA |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2007-09-24 |
Detector | KODAK |
Wavelength(s) | 1.54 |
Spacegroup name | P 63 |
Unit cell lengths | 70.323, 70.323, 104.207 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.228 - 1.800 |
R-factor | 0.179 |
Rwork | 0.177 |
R-free | 0.21800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.294 |
Data reduction software | CrysalisPro |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 24190 | |
<I/σ(I)> | 8.9 | 2.5 |
Completeness [%] | 89.4 | 89.4 |
Redundancy | 7 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 293 | 0.8 to 1M Sodium Citrate, 0.1M Tris, pH 7.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |