3EUU
Crystal structure of the FGFR2 D2 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2006-11-19 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 106.100, 42.460, 79.620 |
Unit cell angles | 90.00, 124.99, 90.00 |
Refinement procedure
Resolution | 22.180 - 2.340 |
R-factor | 0.1858 |
Rwork | 0.184 |
R-free | 0.22772 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3caf |
RMSD bond length | 0.038 |
RMSD bond angle | 2.275 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHASES |
Refinement software | REFMAC (5.3.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.180 | 2.420 |
High resolution limit [Å] | 2.340 | 2.340 |
Rmerge | 0.109 | 0.425 |
Number of reflections | 12416 | |
<I/σ(I)> | 4.9 | 2.2 |
Redundancy | 3.1 | 3.02 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.8M ammonium citrate dibasic, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |