3EUT
X-ray crystal structure of a type III pentaketide synthase from Neurospora crassa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.867, 105.925, 104.124 |
Unit cell angles | 90.00, 90.10, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.000 |
R-factor | 0.17616 |
Rwork | 0.174 |
R-free | 0.22476 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.290 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 25.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 92963 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |