Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-08-03 |
| Detector | SBC-2 |
| Wavelength(s) | 1.0332 |
| Spacegroup name | P 61 |
| Unit cell lengths | 59.340, 59.340, 126.374 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 29.700 - 2.000 |
| R-factor | 0.247 |
| Rwork | 0.225 |
| R-free | 0.25400 |
| Structure solution method | MAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.140 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE (2.06) |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.700 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.045 | 0.275 |
| Number of reflections | 15871 | |
| <I/σ(I)> | 2.813 | |
| Completeness [%] | 93.0 | 63 |
| Redundancy | 6.6 | 4.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 295 | 0.1M Sodium citrate pH 5.6, 0.5M potassium thiocyanate, 5% dioxane, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 295 | 0.1M Sodium citrate pH 5.6, 0.5M potassium thiocyanate, 5% dioxane, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
