3ETI
Structure of a cubic crystal form of X (ADRP) domain from FCoV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-03-13 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.933 |
Spacegroup name | P 21 3 |
Unit cell lengths | 218.990, 218.990, 218.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.800 - 2.200 |
R-factor | 0.149 |
Rwork | 0.147 |
R-free | 0.18100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.020 |
RMSD bond angle | 1.624 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.330 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.154 | 0.607 |
Number of reflections | 176075 | 28013 |
<I/σ(I)> | 20.33 | 5.6 |
Completeness [%] | 99.8 | 98.9 |
Redundancy | 21.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 292 | ammonium citrate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 292K |