Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2005-08-28 |
Detector | NOIR-1 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 65.642, 65.642, 101.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.130 - 1.700 |
R-factor | 0.187 |
Rwork | 0.186 |
R-free | 0.22200 |
Structure solution method | MIR |
RMSD bond length | 0.010 |
RMSD bond angle | 1.137 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.132 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.071 | 0.410 |
Number of reflections | 25076 | |
<I/σ(I)> | 7.6 | 1.6 |
Completeness [%] | 99.8 | 98.3 |
Redundancy | 6.3 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.2M MAGNESIUM CHLORIDE 0.1M TRIS- HCL 30% PEG 4000, PH 8.5, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 295K, pH 8.50 |