3EST
STRUCTURE OF NATIVE PORCINE PANCREATIC ELASTASE AT 1.65 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.100, 58.100, 75.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 * - 1.650 |
Rwork | 0.169 |
RMSD bond length | 0.018 |
RMSD bond angle | 2.500 |
Refinement software | EREF |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.650 * |
Rmerge | 0.093 * |
Number of reflections | 19232 * |
Completeness [%] | 66.0 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | buttom | protein | 5 (%(w/v)) | |
2 | 1 | buttom | sodium acetate | 0.1 (M) | |
3 | 1 | buttom | sodium azide | 0.02 (%(w/v)) | |
4 | 1 | reservoir | sodium sulfate | 0.1 (M) |