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3EN3

Crystal Structure of the GluR4 Ligand-Binding domain in complex with kainate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date2006-03-01
DetectorMAR scanner 345 mm plate
Wavelength(s)1.54
Spacegroup nameC 1 2 1
Unit cell lengths125.906, 48.749, 47.766
Unit cell angles90.00, 109.06, 90.00
Refinement procedure
Resolution11.950 - 2.430
R-factor0.159
Rwork0.156
R-free0.21900
RMSD bond length0.008
RMSD bond angle1.173
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwareCNS
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]11.9502.490
High resolution limit [Å]2.4302.430
Number of reflections10025
Completeness [%]95.394.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.529125.5% PEG 1500, 0.05M Na-Acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K

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