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3EJT

Golgi alpha-Mannosidase II in complex with 5-substituted swainsonine analog:(5R)-5-[2'-(4-tert-butylphenyl)ethyl]-swainsonine

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE A1
Synchrotron siteCHESS
BeamlineA1
Temperature [K]100
Detector technologyCCD
Collection date2005-07-21
DetectorADSC QUANTUM 4
Wavelength(s)0.977
Spacegroup nameP 21 21 21
Unit cell lengths69.372, 110.384, 139.924
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.550 - 1.350
R-factor0.158
Rwork0.158
R-free0.17600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3bub
RMSD bond length0.013
RMSD bond angle1.358
Data reduction softwareHKL-2000
Data scaling softwareSADABS
Phasing softwareCNS
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.370
High resolution limit [Å]1.3501.350
Rmerge0.0820.258
Number of reflections233665
<I/σ(I)>14.715.18
Completeness [%]99.497.3
Redundancy5.964.38
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7298PEG8000, Tris, pH 7, 2.5% MPD, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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