3EIN
Delta class GST
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-27 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 71.775, 63.212, 54.513 |
Unit cell angles | 90.00, 129.84, 90.00 |
Refinement procedure
Resolution | 31.610 - 1.126 |
R-factor | 0.141 |
Rwork | 0.140 |
R-free | 0.15700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.267 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.170 |
High resolution limit [Å] | 1.130 | 1.130 |
Rmerge | 0.048 | 0.196 |
Number of reflections | 69523 | |
Completeness [%] | 99.2 | 94 |
Redundancy | 4 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 294 | 25%(w/v) PEG3350, 0.2M NaCl, 100mM HEPES, pH8.0, VAPOR DIFFUSION, HANGING DROP, temperature 294K |