3EFY

Structure of the Cyclomodulin Cif from Pathogenic Escherichia coli

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X29A
Synchrotron site	NSLS
Beamline	X29A
Temperature [K]	93
Detector technology	CCD
Collection date	2005-04-10
Detector	ADSC QUANTUM 315
Wavelength(s)	1.000
Spacegroup name	P 42 2 2
Unit cell lengths	111.768, 111.768, 107.518
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.330 - 1.700
R-factor	0.18262
Rwork	0.181
R-free	0.22202
Structure solution method	SAD
RMSD bond length	0.018
RMSD bond angle	1.639
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHELXS
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.700
Number of reflections	74589

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	3.8	277.15	1.85M Sodium Malonate, 0.1M tri-sodium citrate dihydrate, pH 3.8, VAPOR DIFFUSION, HANGING DROP, temperature 277.15K