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3EES

Structure of the RNA pyrophosphohydrolase BdRppH

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X6A
Synchrotron siteNSLS
BeamlineX6A
Temperature [K]100
Detector technologyCCD
Collection date2007-04-09
Detectoradsc Q210
Wavelength(s)1.0
Spacegroup nameP 32 2 1
Unit cell lengths70.491, 70.491, 100.481
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution33.260 - 1.900
R-factor0.223
Rwork0.222
R-free0.25600
Structure solution methodMIR
RMSD bond length0.010
RMSD bond angle1.298
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSOLVE (2.03)
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]33.26050.0001.970
High resolution limit [Å]1.9004.0901.900
Rmerge0.0430.0330.390
Number of reflections23316
<I/σ(I)>63.364
Completeness [%]99.898100
Redundancy10109
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1hanging drop4298PEG 4000, Na acetate, hanging drop, temperature 298K

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