3EAI

Structure of inhibited murine iNOS oxygenase domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 4
Spacegroup name	P 61 2 2
Unit cell lengths	213.111, 213.111, 116.562
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.950 - 2.200
Rwork	0.223
RMSD bond length	0.007
RMSD bond angle	1.300
Data reduction software	DENZO
Phasing software	CNS
Refinement software	CNS (1.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.950
High resolution limit [Å]	2.200
Number of reflections	67287

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	298	pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K