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3E7Y

Structure of human insulin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsBRUKER AXS MICROSTAR
Temperature [K]100
Detector technologyCCD
DetectorBRUKER SMART 6000
Spacegroup nameH 3
Unit cell lengths82.810, 82.810, 34.002
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution11.823 - 1.600
R-factor0.171
Rwork0.167
R-free0.21250
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle0.972
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 Overall
Low resolution limit [Å]14.810
High resolution limit [Å]1.600
Number of reflections10856
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1

226707

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