3E7Y
Structure of human insulin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | BRUKER SMART 6000 |
Spacegroup name | H 3 |
Unit cell lengths | 82.810, 82.810, 34.002 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 11.823 - 1.600 |
R-factor | 0.171 |
Rwork | 0.167 |
R-free | 0.21250 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.972 |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 14.810 |
High resolution limit [Å] | 1.600 |
Number of reflections | 10856 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |