3E7Y

Structure of human insulin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	BRUKER AXS MICROSTAR
Temperature [K]	100
Detector technology	CCD
Detector	BRUKER SMART 6000
Spacegroup name	H 3
Unit cell lengths	82.810, 82.810, 34.002
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	11.823 - 1.600
R-factor	0.171
Rwork	0.167
R-free	0.21250
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.972
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	14.810
High resolution limit [Å]	1.600
Number of reflections	10856

Crystallization Conditions

crystal ID	method	pH	temperature	details
1