3E5X
OCPA complexed CprK
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.700, 118.380, 87.460 |
Unit cell angles | 90.00, 95.68, 90.00 |
Refinement procedure
Resolution | 35.940 - 1.999 |
R-factor | 0.19517 |
Rwork | 0.193 |
R-free | 0.23761 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.024 |
RMSD bond angle | 1.903 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.940 |
High resolution limit [Å] | 1.999 |
Number of reflections | 75930 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 277 | 100mM sodium chloride, 100mM sodium acetate, 20% PEG 6000, pH 5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |