3DYU
Crystal structure of Snx9PX-BAR (230-595), H32
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-17 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97710 |
Spacegroup name | H 3 2 |
Unit cell lengths | 131.765, 131.765, 569.072 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.940 - 4.100 |
R-factor | 0.388 |
Rwork | 0.388 |
R-free | 0.40300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 2RAK 3dyt |
RMSD bond length | 0.008 |
RMSD bond angle | 1.500 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 4.250 |
High resolution limit [Å] | 4.100 | 4.100 |
Rmerge | 0.056 | 0.888 |
Number of reflections | 15467 | |
<I/σ(I)> | 25.9 | 3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.2 | 12.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293.15 | 1.8M Ammonium sulfate, 0.1M Tris-HCl pH 8.5, 5% PEG 400, 0.05M MgSO4, 15% Xylitol, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |