3DYJ
Crystal Structure of the R11R12 Domains of Talin
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-18 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.713, 57.648, 92.547 |
Unit cell angles | 90.00, 102.96, 90.00 |
Refinement procedure
Resolution | 19.570 - 1.850 |
R-factor | 0.215 |
Rwork | 0.214 |
R-free | 0.25989 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.454 |
Data reduction software | DENZO |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 52439 | |
<I/σ(I)> | 16.8 | 1.7 |
Completeness [%] | 98.1 | 87.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 10% PEG 8000, 1% PEG 3350, 100MM HEPES (PH 7.5), 10MM SODIUM THIOCYANATE, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 273K, pH 7.50, temperature 293K |