3DXX
Crystal structure of EcTrmB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-03-18 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.420, 47.010, 58.640 |
Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
Resolution | 24.790 - 2.050 |
R-factor | 0.19457 |
Rwork | 0.193 |
R-free | 0.22687 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.244 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 24.790 |
High resolution limit [Å] | 2.040 |
Number of reflections | 15183 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 283 | 15% (w/v) PEG 3350, 150mM MgSO4, VAPOR DIFFUSION, HANGING DROP, temperature 283K |