3DX9
Crystal Structure of the DM1 TCR at 2.75A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-18 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.740, 70.727, 154.412 |
Unit cell angles | 90.00, 94.69, 90.00 |
Refinement procedure
Resolution | 154.300 - 2.750 |
R-factor | 0.207 |
Rwork | 0.204 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.490 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 154.300 |
High resolution limit [Å] | 2.750 |
Number of reflections | 22674 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Hepes, Magnesium Formate, PEG 3350, pH 7.0, vapor diffusion, hanging drop, temperature 293K |