3DU6
Structure of the catalytic subunit of telomerase, TERT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 298 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 85.042, 122.657, 212.406 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.710 |
R-factor | 0.24038 |
Rwork | 0.238 |
R-free | 0.27763 |
Structure solution method | SIRAS |
RMSD bond length | 0.007 |
RMSD bond angle | 0.848 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.710 |
Number of reflections | 56173 |
<I/σ(I)> | 9.3 |
Completeness [%] | 97.0 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |