3DPA

CRYSTAL STRUCTURE OF CHAPERONE PROTEIN PAPD REVEALS AN IMMUNOGLOBULIN FOLD

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	58.200, 64.000, 67.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.500
R-factor	0.184 *
Rwork	0.184
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.053 *
Total number of observations	20920 *
Number of reflections	6353 *
Completeness [%]	69.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	12 (mg/ml)
2	1	reservoir	PEG8000	15 (%)