3DNB
HELIX GEOMETRY, HYDRATION, AND G.A MISMATCH IN A B-DNA DECAMER
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Detector technology | DIFFRACTOMETER |
Detector | NICOLET P1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 32.520, 26.170, 34.300 |
Unit cell angles | 90.00, 118.90, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.300 |
R-factor | 0.164 |
RMSD bond length | 0.019 |
RMSD bond angle | 0.027 * |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 1.300 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | VAPOR DIFFUSION, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | MGCL2 | ||
4 | 1 | 2 | WATER | ||
5 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 9 (mg/ml) | |
2 | 1 | drop | 0.7 (M) | ||
3 | 1 | reservoir | MPD | 45 (%(v/v)) |