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3DKS

DsbA substrate complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-BM-C
Synchrotron siteAPS
Beamline14-BM-C
Temperature [K]113
Detector technologyIMAGE PLATE
Collection date2005-11-09
DetectorRIGAKU RAXIS
Spacegroup nameP 21 21 21
Unit cell lengths85.433, 87.938, 112.566
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution69.340 - 1.900
R-factor0.217
Rwork0.217
R-free0.25200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1dsb
RMSD bond length0.009
RMSD bond angle1.020
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]69.340
High resolution limit [Å]1.9001.900
Number of reflections67234
<I/σ(I)>15.8
Completeness [%]99.8
Redundancy7.16.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.7277.150.2M AMMONIUM ACETATE, 20%(W/V) PEG 4000, 0.1M sodium citrate(pH 5.8), pH 6.700000, VAPOR DIFFUSION, HANGING DROP, temperature 277.15K

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