3DKM
Crystal structure of the HECTD1 CPH domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-06-01 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.710, 45.564, 51.101 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.100 - 1.600 |
R-factor | 0.15695 |
Rwork | 0.156 |
R-free | 0.17788 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dk3 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.620 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 10709 | |
<I/σ(I)> | 40.84 | 11.103 |
Completeness [%] | 98.1 | 87.1 |
Redundancy | 9.7 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 20 % PEG 5000, 0.1 M BIS-TRIS, PH 6.50, VAPOR DIFFUSION, SITTING DROP, temperature 298K |