3DJ4
Crystal Structure of GlmU from Mycobacterium tuberculosis in complex with URIDINE-DIPHOSPHATE-N-ACETYLGLUCOSAMINE.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54179 |
Spacegroup name | H 3 |
Unit cell lengths | 78.600, 78.600, 278.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.030 - 2.380 |
R-factor | 0.197 |
Rwork | 0.194 |
R-free | 0.25700 |
RMSD bond length | 0.027 |
RMSD bond angle | 2.544 |
Data scaling software | XSCALE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.440 | |
High resolution limit [Å] | 2.380 | 2.380 |
Rmerge | 0.097 | 0.443 |
Number of reflections | 25334 | 1553 |
<I/σ(I)> | 19.84 | 4.3 |
Completeness [%] | 98.3 | 82.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 8% PEG 8000, 150mM NaCl, 2mM MnCl2, 5% Glycerol, 1,3-butanediol, AMPPNP, MgCl2, DTT, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |