3DIH
Crystal structure of ammodytin L
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1994-08-17 |
Detector | ENRAF-NONIUS FAST |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 2 |
Unit cell lengths | 120.500, 120.500, 63.150 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 21.340 - 2.600 |
R-factor | 0.159 |
Rwork | 0.156 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.190 |
RMSD bond angle | 2.000 |
Data reduction software | MOSFLM |
Data scaling software | rotavata/agrovata |
Phasing software | AMoRE |
Refinement software | MAIN |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.800 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 5349 | |
<I/σ(I)> | 7.7 | 2.8 |
Completeness [%] | 96.9 | 94.4 |
Redundancy | 5.8 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | 0.2M glycine, pH 9, 1M NaCl, VAPOR DIFFUSION, SITTING DROP, temperature 293K |