3DI5
Crystal structure of a dinb-like protein (bce_4655) from bacillus cereus atcc 10987 at 2.01 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-10 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837,0.97916,0.97860 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 78.120, 84.190, 50.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.630 - 2.009 |
R-factor | 0.231 |
Rwork | 0.229 |
R-free | 0.26600 |
Structure solution method | MAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.273 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.630 | 28.630 | 2.070 |
High resolution limit [Å] | 2.009 | 4.300 | 2.000 |
Rmerge | 0.034 | 0.021 | 0.413 |
Number of reflections | 11180 | 2093 | 1627 |
<I/σ(I)> | 13.57 | 32.1 | 2.63 |
Completeness [%] | 95.6 | 95.7 | 77.6 |
Redundancy | 3.93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.57 | 293 | 0.2M magnesium chloride, 30.5% polyethylene glycol 4000, 0.1M TRIS pH 8.57, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 293K |