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3DD7

Structure of DocH66Y in complex with the C-terminal domain of Phd

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE X12
Synchrotron siteEMBL/DESY, HAMBURG
BeamlineX12
Temperature [K]100
Detector technologyCCD
Collection date2007-04-19
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)0.9189, 0.9116
Spacegroup nameC 1 2 1
Unit cell lengths110.944, 38.201, 63.734
Unit cell angles90.00, 99.26, 90.00
Refinement procedure
Resolution11.000 - 1.700
R-factor0.18317
Rwork0.182
R-free0.19849
Structure solution methodMAD
RMSD bond length0.011
RMSD bond angle1.237
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAuto-Rickshaw
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]11.0001.760
High resolution limit [Å]1.7001.700
Rmerge0.0900.950
Number of reflections29371
<I/σ(I)>92
Redundancy7.14.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.629335% PEG4000, 0.2M ammonium acetate, 0.1M acetate, pH4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K

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