Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X13 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-05-08 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.8073 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 106.644, 106.644, 311.667 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.490 |
| R-factor | 0.18388 |
| Rwork | 0.182 |
| R-free | 0.22379 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1m2t |
| RMSD bond length | 0.022 |
| RMSD bond angle | 2.082 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | |
| High resolution limit [Å] | 2.490 | 2.490 |
| Rmerge | 0.075 | 0.620 |
| Number of reflections | 37504 | |
| <I/σ(I)> | 3.9 | |
| Redundancy | 10.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIQUID DIFFUSION | 2.5 | 293 | counter diffusion under microgravity conditions during JAXA-GCF-flight number 6, pH 2.5, LIQUID DIFFUSION, temperature 293K |
