3D3J
Crystal structure of human Edc3p
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-10 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 119.741, 119.741, 93.923 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.23197 |
Rwork | 0.229 |
R-free | 0.29062 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3d3k |
RMSD bond length | 0.006 |
RMSD bond angle | 0.978 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.800 |
Number of reflections | 9673 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG 6000, sodium cacodylate, magnesium acetate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |