3D34
Structure of the F-spondin domain of mindin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.600, 68.027, 110.130 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 1.800 |
Rwork | 0.189 |
R-free | 0.21500 |
Data reduction software | DENZO |
Data scaling software | d*TREK (9.2SSI) |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.730 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.052 | 0.163 |
Total number of observations | 9255 | |
Number of reflections | 35173 | |
<I/σ(I)> | 13.5 | 5.8 |
Completeness [%] | 97.3 | 93.7 |
Redundancy | 3.08 | 2.96 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 298 | 0-6% PEG2000, 100mM Tris-HCl, 10mM NiCl2, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |