3D2N
Crystal structure of MBNL1 tandem zinc finger 1 and 2 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-10-27 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.2821 |
Spacegroup name | P 31 |
Unit cell lengths | 49.320, 49.320, 36.026 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.700 |
R-factor | 0.23284 |
Rwork | 0.230 |
R-free | 0.27942 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.579 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 5336 | |
<I/σ(I)> | 2.7 | |
Completeness [%] | 98.7 | 90.1 |
Redundancy | 2.9 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.2 | 277 | 20% PEG 4000, 0.1M sodium citrate, 20 % isopropanol, pH 7.2, VAPOR DIFFUSION, temperature 277K |