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3D26

Norwalk P domain A-trisaccharide complex

Replaces:  3BY3
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2007-10-29
DetectorRIGAKU RAXIS IV++
Spacegroup nameP 31 2 1
Unit cell lengths83.010, 83.010, 162.979
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution50.000 - 2.300
R-factor0.22
Rwork0.220
R-free0.26000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ihm
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.000
High resolution limit [Å]2.3002.300
Number of reflections23678
Redundancy3.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.529513% (w/v) PEG 4000, 0.2 M (NH4)2SO4, 0. 1 M NaOAc, pH 4.50, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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