Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1993-11 |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 62.710, 62.710, 111.090 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.600 |
R-factor | 0.166 * |
R-free | 0.22100 |
Structure solution method | RIGID-BODY REFINEMENT |
Starting model (for MR) | 2CYR |
RMSD bond length | 0.031 |
RMSD bond angle | 2.874 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((AGROVATA) |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.800 | 1.680 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.063 | 0.305 |
Total number of observations | 88838 * | |
Number of reflections | 17593 | |
<I/σ(I)> | 8.7 | 2.4 |
Completeness [%] | 99.1 | 98.4 |
Redundancy | 5.1 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | 4 | Matias, P.M., (1993) J. Mol. Biol., 234, 680. * |