3CXR
Crystal structure of gluconate 5-dehydrogase from streptococcus suis type 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 71.147, 75.378, 97.674 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.560 - 2.000 |
| R-factor | 0.19193 |
| Rwork | 0.191 |
| R-free | 0.20772 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1vl8 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.243 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.660 | 30.560 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 19757 | |
| <I/σ(I)> | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
