3CXR
Crystal structure of gluconate 5-dehydrogase from streptococcus suis type 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 71.147, 75.378, 97.674 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.560 - 2.000 |
R-factor | 0.19193 |
Rwork | 0.191 |
R-free | 0.20772 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vl8 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.243 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.660 | 30.560 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 19757 | |
<I/σ(I)> | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |