3CWX
Crystal structure of cagd from helicobacter pylori pathogenicity island
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-12-07 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97942, 0.97420, 0.97814 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 78.181, 117.956, 65.157 |
| Unit cell angles | 90.00, 110.26, 90.00 |
Refinement procedure
| Resolution | 62.260 - 2.300 |
| R-factor | 0.242 |
| R-free | 0.28800 |
| Structure solution method | MAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.019 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHARP |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 62.260 | 2.320 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.088 | 0.411 |
| Number of reflections | 28577 | |
| <I/σ(I)> | 16.6 | 4.1 |
| Completeness [%] | 99.2 | 99.9 |
| Redundancy | 7.3 | 7.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 298 | 0.2 M MgGl2, 0.1M Hepes, 20% PEG 6000, pH 7, VAPOR DIFFUSION, temperature 298K |
