3CVD

Regulation of Protein Function: Crystal Packing Interfaces and Conformational Dimerization

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Spacegroup name	P 43 21 2
Unit cell lengths	85.843, 85.843, 90.282
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.770 - 1.500
R-factor	0.155
Rwork	0.153
R-free	0.18400
RMSD bond length	0.014
RMSD bond angle	1.517
Data scaling software	SCALA
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	29.300
High resolution limit [Å]	1.500
Number of reflections	54990

Crystallization Conditions

crystal ID	method	pH	temperature	details
1