3CTW
Crystal Structure of RcdA from Caulobacter crescentus CB15
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Detector technology | CCD |
Collection date | 2007-08-26 |
Detector | ADSC Q315 |
Wavelength(s) | 0.97957,1.01986,0.97972 |
Spacegroup name | P 43 |
Unit cell lengths | 75.458, 75.458, 81.419 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.630 - 2.900 |
R-factor | 0.276 |
Rwork | 0.274 |
R-free | 0.31200 |
Structure solution method | MAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.645 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC (5.4.0067) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 6.030 | 2.800 |
Rmerge | 0.099 | 0.039 | 0.458 |
Number of reflections | 10955 | ||
<I/σ(I)> | 7.5 | ||
Completeness [%] | 96.9 | 100 | 75.4 |
Redundancy | 4.8 | 4.8 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 100mM HEPES, 1.75M Formate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 100mM HEPES, 1.75M Formate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |