3CT6
Crystal structure of DhaM of L. lactis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X12 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-04-13 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 30.600, 62.400, 69.700 |
Unit cell angles | 90.00, 99.60, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.100 |
R-factor | 0.1468 |
R-free | 0.17690 |
Structure solution method | AB INITIO |
RMSD bond length | 0.022 |
RMSD bond angle | 0.033 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SOLVE (2.08) |
Refinement software | SHELX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.136 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.069 | 0.253 |
Number of reflections | 97245 | |
<I/σ(I)> | 17.41 | 4.4 |
Completeness [%] | 93.0 | 90.77 |
Redundancy | 2.489 | 2.218 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 2.8 | 289 | 200 mM NaNO3, 20 % PEG 3350, pH 2.8, VAPOR DIFFUSION, SITTING DROP, temperature 289K |