3CRB
Crystal structure of the complex of C-lobe of lactoferrin with 2-chromenone at 2.6 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 300 |
Detector technology | IMAGE PLATE |
Collection date | 2008-03-26 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.370, 50.370, 65.840 |
Unit cell angles | 90.00, 107.81, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.600 |
R-factor | 0.188 |
Rwork | 0.183 |
R-free | 0.21150 |
Structure solution method | MOLREP |
Starting model (for MR) | 2dyx |
RMSD bond length | 0.010 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 10726 | |
<I/σ(I)> | 5.7 | 2.1 |
Completeness [%] | 86.8 | 92.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 01M ZNSO4, 0.1M MES, 25% PEG, MONOETHYL ETHER 550, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |