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3CR3

Structure of a transient complex between Dha-kinase subunits DhaM and DhaL from Lactococcus lactis

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE X12
Synchrotron siteEMBL/DESY, Hamburg
BeamlineX12
Temperature [K]100
Detector technologyCCD
Collection date2006-12-08
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)0.97885,0.97823,0.97240
Spacegroup nameP 21 21 2
Unit cell lengths74.133, 146.842, 58.483
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution66.230 - 2.100
R-factor0.22168
Rwork0.219
R-free0.26300
Structure solution methodMAD
RMSD bond length0.011
RMSD bond angle1.215
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareSHARP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]147.4422.210
High resolution limit [Å]2.1002.100
Rmerge0.0470.161
Number of reflections37982
<I/σ(I)>22.28.1
Completeness [%]99.824.4
Redundancy4.94.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52890.1 M Tris/HCl, 0.2 M LiSO4, 36 % PEG 4000, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 289K

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