3CNR
Crystal Structure of PilZ (XAC1133) from Xanthomonas axonopodis pv citri
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | LNLS BEAMLINE W01B-MX2 |
Synchrotron site | LNLS |
Beamline | W01B-MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-11-01 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.978294, 0.978581, 0.953724 |
Spacegroup name | P 61 |
Unit cell lengths | 62.125, 62.125, 83.543 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.000 - 1.900 |
R-factor | 0.19285 |
Rwork | 0.190 |
R-free | 0.24345 |
Structure solution method | MAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.547 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.086 | 0.601 |
Number of reflections | 13687 | |
<I/σ(I)> | 24.7 | 1.74 |
Completeness [%] | 99.0 | 92.1 |
Redundancy | 10.7 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | 24% PEG 4000, 0.1 M Tris-HCl, 0.2 M magnesium chloride, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 291K |