3CLP
M. loti cyclic-nucleotide binding domain mutant 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Collection date | 2003-02-09 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.535, 82.011, 50.119 |
Unit cell angles | 90.00, 103.64, 90.00 |
Refinement procedure
Resolution | 48.680 - 2.000 |
R-factor | 0.21286 |
Rwork | 0.212 |
R-free | 0.22938 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.221 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.300 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.038 | |
Number of reflections | 16473 | |
<I/σ(I)> | 8 | |
Completeness [%] | 97.5 | 97.5 |
Redundancy | 4 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |