3CJJ
Crystal structure of human rage ligand-binding domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-21 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.008, 1.28, 1.283 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 74.850, 119.960, 28.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.000 - 1.850 |
R-factor | 0.21 |
Rwork | 0.209 |
R-free | 0.24000 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.988 |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 35.180 | 35.180 | 2.000 |
High resolution limit [Å] | 1.850 | 10.000 | 1.850 |
Rmerge | 0.090 | 0.041 | 0.589 |
Number of reflections | 23066 | 143 | 4712 |
<I/σ(I)> | 11.38 | 19.9 | 3.2 |
Completeness [%] | 99.8 | 77.3 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 0.1M Na cacodylate, 0.2M Zn acetate, 11% PEG 8000, pH 6.5, vapor diffusion, hanging drop, temperature 298K |