3CJH
Tim8-Tim13 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-01-17 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 |
Unit cell lengths | 55.655, 56.303, 59.837 |
Unit cell angles | 89.18, 89.65, 60.30 |
Refinement procedure
Resolution | 19.940 - 2.600 |
R-factor | 0.24691 |
Rwork | 0.244 |
R-free | 0.28884 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.320 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.110 | 0.378 |
Number of reflections | 19026 | |
<I/σ(I)> | 10 | |
Completeness [%] | 96.0 | 94.1 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 298 | 10 mM Tris, pH 8.0, 10 mM NaCl, 3% 2-methyl-2,4-pentanediol (MPD), VAPOR DIFFUSION, SITTING DROP, temperature 298K |